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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925 798-1620 Fax 925-798-1622 <br /> _- - - —- - -- -- _ -W---- — - �Webgue www mceampbeli corn E mail mamQmccampbell com <br /> Advanced GcoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20104-01122/04 <br /> ,0 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> _ <br /> Client P O Date Analyzed 01/24104-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> =E,,1.c1*. d SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-013A <br /> _ - Client ID -- - -P39-45' <br /> Matrix Sot] <br /> orting <br /> Compound Concentration* DF R`L°mt Compound Concentration * DF a`Law <br /> Acenaphthene ND 1 0 0 33 Acenaphthylene ND 1 0 033 <br /> Acetochlor ND _10 033 Anthracene ND 10 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND 10 l 6 <br /> Benzo(a)anthracene ND l 0 0 33-1 Benzo b fluoranthene ND 1 0 033 <br /> Benzo k fluoranthene ND 1 0 033 Benzo( ,h i)perylene ND !0 033 <br /> Benzo(a)pyrene ND 1 0 1 033 Benzyl Alcohol ND l 0 016 <br /> Bis(2-chloreethoxy)Methane ND 1 0 033 Bis(2-chloroeth 1)Ether ND 1 0 033 <br /> Bis(2-chloroisopro l)Ether ND 1 0 033 Bis(2-eth Ihcx l)Adipate ND 1 0 033 <br /> Bis 2-eth lhex 1 Phthalate ND l 0 033 4-Bromo hen l Phenyl Ether ND 10 033 <br /> Bu ]ben t Phthalate ND 1 0 033 4-Chloroanihne ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-meth 1 henol ND 10 —033 <br /> 2-Chlorona hthalene ND 10 033 2-Chlorophenol ND 1 0 033 <br /> 4-Cblorophenyl Phenyl Ether ND 1 0 033 Chrysene ND 1 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-bu i Phthalate ND 10 033 1,2-Dichlorobenzene ND 10 033 <br /> 1 3-Dichlorobenzene ND l 0 0 33 1,4-Dichlorobenzene ND 1 0 033 <br /> • 3,3-Dichlorobenzidme ND 10 066 2,4-Dichloropbenol ND to 033 <br /> Dicthyl Phthalate ND 10 033 2 4-Dimeth I hent ND l 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dinitro-2-meth 1 henol ND 1 0 1 6 <br /> 2,4-Dimtro henol ND 1 0 1 6 2,4-Dinitrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-oct I Phthalate ND 1 0 033 <br /> 1,2-Dr henylh drazmc ND l 0 033 Fluoranthene ND 1 0 033 <br /> Fluorcne ND 10 033 Hexachlorobenzene ND __LO_ 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexach lorocyclopentadiene ND 1 0 1 6 <br /> Hexachloroethane ND 10 033 ]adeno(1,2,3 cd)pyrene ND 1 0 ; 033 <br /> Iso horone ND 10 033 2-Meth !na hthalene ND 1 0 033 <br /> 2-Meth 1 henol(o-Cresol) ND l 0 0 33 3&/or 4-Methylpheno!(m, -Cresol ND 1 0 033 <br /> Naphthalene ND 10 033 2-Nitreaniline ND 1 0 1 6 <br /> 3-Nitroaniline ND 10 16 4-Nitroaniline ND 10 16 <br /> 2-Nitro henol ND 10 16 4-Nitrophenol ND l 0 033 <br /> N-Nitrosodi hen larnine ND 10 033 N-Nitrosodi-n-propylarninc ND 1 0 033 <br /> Pentachlorophenol ND 10 1 6 Phenanthrene ND 1 0 033 <br /> Phenol ND 10 0 33 Pyrene ND 10 033 <br /> 1,2,4-Trichlarobenzene ND 1 0 033 2,4,5-Trichlorophenol ND 10 1 033 <br /> 2,4.6-Trichlorophenol ND 1 0 033 <br /> Surrogate Recoveries(%) <br /> %SSI 946 %SS2 928 <br /> %SS3 86 1 %SS4 869 <br /> %SS5 923 %SS6 874 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludgelsolid samples in mg/kg,wipe samples inµ&/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #)surrogate diluted out of range &)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than–2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCSILCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 �� Angela RydeIius, Lab Manager <br />