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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925 798-1620 Fax 925-798-1622 <br /> 24— _ -- --------W--T--_ — -- ——�-Webvte www mccampbell com E-mail mam gniccampbeil cam------ -- -_ <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 03/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> rClicntt P O Date Analyzed 01124104-01/28/04 <br /> Seirii-Volatile Organics by GC/MS(Basic Target List)* <br /> =C111-t... <br /> d SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-014A <br /> -Client ID = - P40A-15' - - - - — <br /> Matrix Soil <br /> Compound Concentration * DF R�s Compound Concentration * DF a 7 <br /> Acenaphthene I ND 10 1 033 -Acenaphthylene ND 10 0 33 <br /> Acetochlor ND 1 0 033 Anthracene ND <br /> 10 033 <br /> Benzidine ND 10 16 Benzoic Acid ND to 1 6 <br /> Benzo{a anthracene ND 1 0 033 Benzo fluoranthcne ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo( ,h,i)pa lene ND 1 0 033 <br /> Benzo a ne ND 1 10 033 Benal Alcohol ND 1-0 0 66 <br /> Bis(2-chloroethox Methane ND 1 0 033 Bis 2 chloroeth I Ether ND 1 0 033 <br /> Bis(2-chlomiso rop l)Ether ND T 1 0 033 Bis(2-eth ihex l)Adipate ND 1 0--J 033 <br /> Bis 2�th lhex 1 Phthalate ND 1 0 033 4-Bromo hen I Phenyl Ether ND 1 0 0 33 <br /> But lbenz l Phthalate ND 1 0 033 4-Chloroanilrne ND 1 0 1 066 <br /> Nitrobenzene ND 1 D 1 6 4-Chloro-3-meth 1 henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 1 0 0 33 2-Chlorophenol ND 1 0 033 <br /> 4-Chlorophenyl Phen 1 Ethe• ND 10 033 Ch Bene ND 1 0 033 <br /> Dibenzo a h anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Dt-n-but l Phthalate ND 1 0 033 1,2-Dichlorobenzene ND I 10 033 <br /> 1,3-13iichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichlorobenzidme ND 1 0 066 2 4-Dichloro henol ND 1 0 033 <br /> Diethyl Phthalate ND T 1 0 0 33 2,4-Drmethy! henol ND 1 0 033 <br /> Dimeth 1 Phthalate ND 1 10 0 33 4,6-Dinitro-2-meth 1 henol ND l 0 1 6 <br /> 2 4-Dinitro henol ND 1 0 1 6 2,4-Dinttrotoluene ND 1 0 033 <br /> 2 6-Dinitrotoluene ND 1 0 033 Di-n-oct i Phthalate ND 1 0 033 <br /> 1,2-Diphenylhydrazine ND 1 0 033 Fluoranthene ND 1 0 1 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clo entadiene ND 1 0 1 6 <br /> Ilexachloroethane ND 1 0 033 Indeno 1,2,3-cdpyrene ND t 0 0 33 <br /> iso horone ND 1 0 033 2-Methylnaphthalene PTD 1 0 033 <br /> 2-Methylphenol(o-Cresol) ND 1 0 033 3&/or 4-Meth 1phenol(m, -Cresol) ND 1 0 033 <br /> Naphthalene ND 1 0 033 2-Nitroanilme ND 1 0 16 <br /> 3-Nitroamline ND 10 16 4-Nitroanilme ND 10 16 <br /> 2-Nitrophenol ND 1 0 16 i 4-Nitrophenol ND 10 033 <br /> N-Nitrosodi hen lamine ND 1 1 0 033 1 N-Nitrosodi-n-propylarnine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 1 0 033 <br /> Phenol ND l 0 033 Pyrene ND 1 0 033 <br /> !,2,4-Trichlorobenzene ND 10 033 2,4,5-Tncbloro henol ND 1 0 033 <br /> 2 4 6-Trichloro henol ND 1 0 033 <br /> Surrogate Recoveries(%) <br /> %SS] 106 %SS2 108 <br /> %SS3 899 %SS4 930 <br /> %SS5 928 %SS6 979 <br /> Comments <br /> *water samples and ail TCLP&SPLP extracts are reported in pg/L,soil sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/oiunon- <br /> aqueous liquid samples in rng/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 �VAngela Rydeltus, Lab Manager <br />