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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone : 925-798-I620 Fax :925-798-1622 <br />' http://'www.mccaml2bell.com E-mail: main@mccampbell.com <br /> i <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton, CA 95215 Client Contact: Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client P.O: Date Analyzed: 03/16.03/20/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> - Lab ID 62946 <br />' Client ID MW2/03-14-01 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br />' w S W S <br /> Acetone(e) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bmmobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride"' ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide - ND LO 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br />' Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Hther(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 u-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether` ND 1.0 5.0 P1,2,3-Trichlorobertzene <br /> ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 hloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 SA hloroethane ND 1.0 5.0 <br /> 2 Chlarotoluene ND 1.0 5.0 hene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 , , robenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br />' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br />' I,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> I,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.o 5.0 Vinyl Chloride " ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 DibrorrMOfluoromethane 108 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluenc-d8 96 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> • pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol. % <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; { methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chlotoethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />