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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone.925-798-1620 Fax:925-798-1622 <br /> h"://www.mccampbell.com E-mail:main@mccampbell.com <br /> I <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> I <br /> 837 Slaw Road Date Received: 03/16/01 <br /> Stockton, CA 95215 Client Contact: Brian Millman Date Extracted: 03/16-03/20/01 <br /> i <br /> I <br /> Client P.O: Date Analyzed: 03116-03/20/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62947 <br /> Client ID MW3I03-14-01 <br /> Matrix W <br /> Compound Concentration' Reporting Limit Compound Concentration* xtponing Limit <br /> W S W S <br /> Acetone(b) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane ND 1.0 5.0 Hexachlombutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 lodomethane ND 1.0 1 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND I"0 5.0 p-Isopropyl toluene ND IA 5.0 <br /> n-Butyl benzene ND Lo 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.4 5.0 Methylene Chloride` ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone x ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) -- 1.0 5.0 <br /> 10 Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chlomethyl Vinyl Ether` ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform i ND 1.0 5.0 1,10,2-Tetrachloroethane ND 1"0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.4 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> I,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane 15 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5"0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ND 1.4 5.0 <br /> trans-1,2-Dichloroetbene ND 1.0 5.0 Xylenes,total ND 1.4 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 108 <br /> I,1-Dichloropropene ND 1.0 5.0 Toluene-d8 96 <br /> cis-1,3-Dichloropropene ND 1,0 5.0 4-Bromofluorobenzene 94 <br /> 'water and vapor samples are reported in ug(L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (Q 2-butanone; (g) 47methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />