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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htW://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnviromnental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br /> IStockton,CA 95215 Client Contact: Brian Millman Date Extracted: 03/16-03/26/01 <br /> Client P.O: Date Analyzed: 03116-03/26/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62948 <br />' Client ID MW4/03-14-01 <br /> Matrix W <br /> Compound Concentration* <br /> Cirpomng Limit Reporting Limit <br /> W S Compound Concentration* W S <br /> Acetone ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene 16 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane ND l.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichlorornethane ND 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride"' ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> lie Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br />' 2-Chloroethyl Vinyl Ethe ` ND 1.0 5.0 Styrene W ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND- 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br />' 1,2-Dichlorobenzenc ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzenc ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br />' <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane 19 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND l.0 5.0 Vinyl Acetate r3l ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> I trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND t.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromafluoromethane 109 <br />' I,1-Dichloropropene ND 1.0 5.0 Toluene-d8 93 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromolluorobenzene 89 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichlorometbane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol. <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; ).methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> I chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />