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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> htti)://www.rnccamEbeiI.com E-mail:main@tnccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Geweke Date Sampled:03/14/01 <br /> 837 Shaw Road Date Received:03/16/01 <br /> Stockton,CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client PA: Date Analyzed: 03/16-03/20/01 <br /> IVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62955 <br />' Client ID MWI1/03-14-01 <br /> Matrix W <br /> Compound Concentration* Reporting Limn Compound Concentration* Reporting Limit <br /> W S W S <br /> Acetone(e) ND 5.0 25 trans-l,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ' ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND L0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-lsopropyl toluene ND 1.0 5.0- <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride° ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone "ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) --- 1.0 5.0 <br /> Cblorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Fthe ` ND 1.0 5.0 Styrene.,. ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ILIND 1.0 5.0 <br />' Dibromochloromethene ND 1.0 5.0 1,2,3-Trichlarobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br />' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichlompropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br />' 1,2-Dichioroethane ND 1.0 5.0 1,3,5-Trimcthylbenzene ND 1.0 5.0 <br /> I,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate"' ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br />' trans-l,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries{%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromotluoromethane 110 <br />' l,I-Dichloropropene ND 1.0 5.0 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 98 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br />' (b) 2-prcpanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> (h)or isopropylacetone; {h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol. <br /> sediment; (j) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />