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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br />' http://www.mccamt)beil.com E-mail.main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID:Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton, CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03120101 <br /> Client P.O: Date Analyzed: 03116-03/20/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62956 - <br />' Client ID MWI2103-14-01 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporong Limit <br /> W s w s <br />' Acetone ND 5.0 25 bans-l,3-Dichiornpropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5A <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlarobutadiene ND 5.0 25 <br /> Bromodichloromethane ND, 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p4sopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide Nil 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> l <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> ie Chlorobenzenc ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethe ` ND 1.0 5.0 Styrene ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.6 5.0 Tetracbloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-1)ibromo-3-chlompropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br />' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND, 1.0 5.0 <br />' 1,2-Dichloroethane 2.8 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> trans-l,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br />' 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND ±J05.0 Surrogate Recoveries(%)2,2-Dichloropropane ND Dibromotluoromethane 110 <br /> I,1-Dichloropropene ND Toluene-dS 95 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 97 <br /> `water and vapor samples are reported in ug/L,soii'and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br />' (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br />' DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />