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1 Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> i <br /> Dite Work Order <br /> ' 02-May-03 QC Summary Report 03042224 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS091DATA1030423403042307 D Batch ID MS9SO423A Analysis Date 04123/2003 11 47 <br /> ' Sample ID MBLK MS9SO423A Units pg/Kg Run ID GCIMSD_9_030423A Prep Date 04/23/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Quat <br /> Chloromethane NO 40 <br /> Vinyl chloride NO 20 <br /> ' Chloroethane NO 20 <br /> Bromomethane NO 20 <br /> Trichlorofluoromethane NO 20 <br /> 11-Dlchloroethene NO 20 <br /> ' Tertiary Butyl Alcohol(TBA) ND 500 <br /> Dichloromethane NO 40 <br /> trans 1 2-Dichloroethene NO 20 <br /> Methyl Cert-butyl ether(MTBE) ND 5 <br /> t11-Dichloroethane ND 20 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> as-1,2-Dichloroethene ND 20 <br /> Chloroform ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) NO 20 <br /> ' 12-Dichloroethane NO 20 <br /> 11,1-Trichloroethane NO 20 <br /> Carbon tetrachloride ND 20 <br /> Benzene NO 5 <br /> Tertiary Amyl Methyl Ether(TAME) NO 20 <br /> 1,2-Dichloropropane ND 20 <br /> Trichloroethene ND 20 <br /> Bromodichloromethane NO 20 <br /> W113-Dichlgropropene NO 20 <br /> s-13-Dichloropropene ND 20 <br /> 2-Trichloroethane NO 20 <br /> Toluene ND 5 <br /> Dibromochloromethane ND 20 <br /> ' <br /> Tetra chloroethene ND 20 <br /> Chlorobenzene NO 20 <br /> Ethylbenzene ND 5 <br /> m p-Xylene ND 5 <br /> Bromoform NO 20 <br /> o-Xylene NO 5 <br /> 1 1 2 2-Tetrachloroethane ND 20 <br /> 13-Dichlorobenzene NO 20 <br /> ' 14-Dichlorobenzene NO 20 <br /> 12-Dichlorobenzene ND 20 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> ' File ID D 1HPCHEM1MS091DATA1030423103042308 D Batch ID MS9SO423A Analysis Date 041231200312 11 <br /> Sample ID LCS MS9SO423A Units pg/Kg Run ID GCIMSD_9_030423A Prep Date 04123/2003 <br /> Analyte Result PQL SpkVal SpkRWal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-DichJoroethene 279 20 200 14 0 147 <br /> Benzene 194 5 200 97 60 142 <br /> Tnchloroethene 196 20 200 98 60 142 <br /> Toluene 200 5 200 100 58 143 <br /> Chlorobenzene 197 20 200 98 57 144 <br /> Ethylbenzene 210 - 5 200 105 58 147 <br /> m p-Xylene 400 5 400 100 57 147 <br /> o-Xylene 195 5 200 98 58 149 <br /> 1 <br /> i <br /> 1 <br /> - 1 <br />