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McCampbell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 14 Web:www.mccampbell.com E-mail:main@mcrzmpbea.com "When Oualiry Comes" I Telephone:877-252-9262 Fax:925-252-9269 NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 Terminal Waste Date Received: 05/05/08 1100 Willow Pass Road Client Contact: Dan Thomas Date Extracted: 05/05/08-05/06/08 Pittsburg,CA 94565 Client P.O.: 44501224877 Date Analyzed 05/08/08 RCRA Metals* Extraction Method: SW 1111 Analytical Method: 6020A work Order: 0805!10 Lab ID 0805110-001A 0805110-002A Client ID 29080312-01 29080312-02 Reporting Limit for Matrix Soil Soil DF=1 DF 1 I Extraction Type TCLP TCLP S W Compound Concentration mg/L pg/L Arsenic ND ND 0.1 NA Barium ND ND 1.0 NA Cadmium ND ND 0.05 NA Chromium ND ND 0.1 NA Lead ND ND 0.1 NA Mercury NO ND 0.01 NA Selenium ND ND 0.1 NA Silver NO ND 0.1 NA Surrogate Recoveries Comments -water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in mg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. q means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or instrument. TOTAL=acid digestion. WET=Waste Extraction Test(STLC). DI WET=Waste Extraction Test using de-ionized water. i)aqueous sample containing greater than—1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for TOTAL^metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery,caused by matrix interference;n)results are reported on a dry weight basis; )see attached narrative. DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager