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i <br /> 1102nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt*y 1/www mccMbell corn E-mail main@mccampbell com <br /> • <br /> IAdvanced GeoEnvironmental Client Protect ID Larrys Auto Date Sampled 06/08/01 <br /> Date Received 06/13/01 <br /> I 837 Shaw Road <br /> Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 06115-06/19/01 <br /> Client F 0 [D�atealyz�dO5-06/19/01 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> I Lab ID 69664 <br /> Client ID VW3/060801 <br /> Matrix W <br /> g�po�t+ng I,�mrt <br /> Compound Concentration* Compound Concentration* W S <br /> Acetone roi ND<1000 trans-l,3-Dichloropropene ND<500 1 0 5 0 <br /> Benzene 32,000Eth lene dibromide ND<500 l 0 5 0 <br /> Bromobenzene ND<500 10150 Ethylbenzene 3300 1 0 5 0 <br />' Bromochloromethane ND<500 llexachlorgbutadiene ND<500 5 0 25 <br /> Bromodichloromethane ND<500 —j-0— 5 0 Iodomethane ND1500 10 5 0 <br /> Bromoform ND<500 FO— 5 0 Isq ropylbenzenc ND<500 10 50 <br /> Bromomethane ND<500 10 5 0 -Iso ropyl toluene ND<500 1 0 50 <br /> n-Butyl benzene ND<500 1 0 5 0 Methyl butyl ketone cel ND<500 10 50 <br /> sec-Butyl benzene ND<500 1 0 5 0 Methylene Chloride' ND<750 10 5 0 <br /> tert-Butyl benzene ND<500 1 0 5 0 Methyl eth1 ketone MND<500 20 10 <br /> Carbon Disulfide ND<500 1 0 50 Msobutyl ketone ND<500 10 5 0 <br /> N Carbon 1 etrachlonde ND<5U0 1 0 5 0 Methyl tert-Bu l Ether(MTBE) -- 10 5 0 <br /> Chlorobenzene ND<500 1 0 5 0 Naphthalene NI3<500 5 0 5 4 <br /> Chloroethane ND<500 1 0 5 0 n-Propyl benzene ND<500 10 50 <br />' 2-Chloroethyl Vinyl Ether" ND<500 10 5 0 Styrene i ND<500 10 50 <br /> Chloroform ND<500 1 0 50 1,1,1,2-Tetrachloroethane ND<500 1 0 50 <br /> Chloromethane ND<500 l 0 5 0 1,1,2,2-Tetrachloroethane ND<S00 1 0 5 0 <br /> 2-Chlorotolucne ND<500 10 5 0 Tetrachloroethane ND<500 1 0 50 <br />' 4-Chlorotoluene ND<500 1 0 50 Toluene i t 11,000 10 5 0 <br /> Dibromochloromethane ND<500 10 50 1,2,3-Trichlorobenzene ND<500 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND<500 2 0 10 1,2,4-Trichlorobenzene ND<500 — 50 25 <br /> Dibromomethane ND<500 1 0 50 1,1,1-Trichloroethane ND<500 10 50 <br />' 1,2-Dichlorobenzene ND<500 1 0 50 1,1 2-Trichloroethane ND<500 10 50 <br /> 1,3-Dichlorobenzene ND<500 to 50 Tnchloroethene ND<500 10 5 0 <br /> 1,4-Dichlorobenzene ND<500 1 0 5 0 Tnchlorofluoromethane ND<500 1 0 5o <br /> Dichlorodifluoromethane ND<500 1 0 —30— 1,2,3-Triebloropropane ND<500 10 5 0 <br />' 1 1-Dichloroethane ND<500 1 0 --570— 1,2,4-Tnmethylbenzene 2100 10 5 0 <br /> 1,2-Dichloroethane ND<500 to 5 0 1,3,5-Tnmethylbenzene 520 10 50 <br /> 1,I-Dichloroethenc ND<500 to 50 Vinyl Acetate c�i ND<500 5 0 25 <br /> cis-1,2-Dichloroethene ND<500 10 5 0 Vinyl Chloride°°i ND<500 1 0 5 0 <br />' trans-l,2-Dichloroethene ND<500 1 0 5 0 Xylenes,total 15,000 1 4 S 0 <br /> 1,2-Dichloropro ane ND<500 1 0 5 0 Comments <br /> 1,3-�Dichloro roane ND<500 10 5 0 Sur ate Recovenes <br /> 2 2-Dichloropropane NDc500 10 5 0 Dibromofluoromethane FF981,1-Dichlororopene ND<500 10 5 0 Toluene-d8 7 <br /> cis-1 3-Dichloro ra ene ND<500 10 5 0 4-Bromofluorobenzene 108 <br /> 'water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ugtL <br />' ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br />' chioroethene, o dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />