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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> //www E-mail mam@mccampbell com <br />' Advanced GeoEnvironmental Client Protect ID Larry's Auto Repair Date Sampled 11/22/99 <br /> 4005 North Wilson Way Date Received 11/23/99 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/23-11/30199 <br /> Client P O Date Analyzed 11123-11130/99 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br />' <br /> Lab ID 26116 <br /> Client 1D MW-7/11-22-99 <br /> Matnx W <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<7 0 trans-l,3-Dichloropropene ND<2 5 <br /> Benzene 24 Ethylene dibromide ND<2 5 <br /> Bromobenzenc ND<2 5 Ethylbenzene 11 <br /> Bromochloromethane ND<2 5 Hexachlorobotadiene NIX2 5 <br />' Bromodichloromethane ND<2 5 lodomethane ND<2 5 <br /> Bromoform ND<2 5 Isopropylbenzene 38 <br /> Bromomethane ND<2 5 p-Isopropyl toluene N1<2 5 <br /> n-Butyl benzene ND<2 5 Methyl butyl ketone ND<2 5 <br />' sec-Butyl benzene ND<2 5 Methylene Chloride"' ND<2 5 <br /> tert-Butyl benzene ND<2 5 Metbyi ethyl ketone ND<2 5 <br /> Carbon Disulfide ND<2 5 Methyl isobutyl ketone ND<2 5 <br /> Carbon Tetrachloride ND<2 5 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzcnc ND<2 5 Naphthalene N0<2 5 <br /> Chloroethane ND<2 5 n-Propyl benzene ND<2 5 <br /> 2-Chloroethyl Vinyl Ether" ND<2 5 Styrene ND<2 5 <br />' Chloroform 9 0 1,1,1,2-Tetrachloroethane ND<2 5 <br /> Chloromethane ND<2 5 1,1,2,2-Tetrachloroethane ND<2 5 <br /> 2-Chlorotoluene ND<2 5 Tetrach]oroethene ND<2 5 <br /> 4-Chlorotoluene ND<2 5 Toluene m 21 <br />' Dibromoch]oromethane ND<2 5 1,2,3-Tnchlorobenzene ND4 5 <br /> 1,2-Dibromo-3-chloropropane NIX2 5 1,2,4-Tnchlorobenzene ND<2 5 <br /> Dibromomethane ND<2 5 1,1,1-Tnchloroethane ND<2 5 <br /> 1,2 Dichlorobenzene ND<2 5 1,1,2 Trichloroethane ND<2 5 <br />' 1 3-Dichlorobenzene ND<2 5 Trichloroethene ND<2 5 <br /> 1,4 Dichlorobenzene ND<2 5 Trichlorofluoromethane ND<2 5 <br /> Dichlorodifluoromethane ND<2 5 1,2,3-Tnchloropropane ND<2 5 <br /> 1,1 Dlchlor0ethane ND<2 5 1,2,4-Tnmethylbenzene 9 9 <br />' 1,2 Dichloroethane NDQ 5 1,3,5-Tntnethylbenzene ND<2 5 <br /> l,l-Dichloroethane ND<2 5 Vinyl Acetate"I ND<2 5 <br /> cis-1,2 Dichloroethene ND<2 5 Vinyl Chloride ° ND<2 5 <br /> trans-1,2-Dichloroethene ND<2 5 Xylenes,total 34 <br />' 1,2-Dichloropropane ND<2 5 Comments <br /> 1,3 Dichloropropane ND<2 5 Surrogate Rem%tries(%) <br /> 2 2-Dichloropropane ND<2 5 Dibromofluoromethane 97 <br /> 1,1-Dichloropropene ND<2 5 Toluene-d8 101 <br />' cis 1,3-Dichloropropene ND<2 5 4-Bromofluorobcnzene 88 <br /> uater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,Wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated eater samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,w'Ipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable 10 this analysis <br /> (b) 2-propanonc or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, p) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethane (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />