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I <br /> 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ham]//www mccarnnbell co m E-mail mam@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Repair Date Sampled 11/22/99 <br /> 4005 North Wilson Way Date Received 11/23/99 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11123-11/30199 <br /> Client P O Date Analyzed 11123-11/30/99 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br />' Lab ID 26117 <br /> Client ID VW-213/11-22-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone i ND<500 trans-l,3-Diehl oropropene ND<500 <br /> Benzene 29,000 Ethylene dibromide ND<500 <br /> Bromobenzene ND<500 Ethylbenzene 3000 <br /> Bromochloromethane ND<500 Hexachlorobutadiene ND<500 <br /> Bromodichloromethane ND<500 Iodomethane ND<500 <br /> Bromoform ND<500 Isopropylbenzene NIX500 <br /> Bromomethane ND<500 p-Isopropyl toluene ND<500 <br /> n-Butyl benzene ND<500 Methyl butyl ketone ' ND<500 <br />' sec-Butyl benzene ND<500 Methylene Chloride" ND<540 <br /> tert-Butyl benzene ND<500 Methyl ethyl ketone ND<500 <br /> Carbon Disulfide ND<500 Methyl isobutyl ketone a ND<500 <br /> Carbon Tetrachloride ND<500 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<500 Naphthalene ND<500 <br /> Chloroethane ND<500 n-Propyl benzene ND<500 <br /> 2-Chloroethyl Vinyl Ether") ND<500 Styrene ND<500 <br />' Chloroform ND<500 1,1,1,2-Tetrachloroethane ND<500 <br /> Chloromethane ND<500 1,1,2,2-Tetrachloroethane ND<500 <br /> 2-Chlorotoluene ND<500 Tetrachloroethene ND<500 <br /> 4-Chlorotoluene ND<500 Toluene"1 23,000 <br />' Drbromochloromethane ND<500 1,2,3-Tnchlorobenzene ND<500 <br /> 1,2-Dibromo-3-chloropropane ND<500 1,2,4-Tnchlorobenzene NIX500 <br /> Dibromomethane ND<500 1,1,1-Tnchloroethane ND<500 <br /> 1,2-Dichlorobenzene ND<500 1,1,2-Tnchloroethane ND<500 <br /> 1,3-Dichlorobenzene ND<500 Trichloroethene ND<500 <br /> 1,4-Dichlorobenzene ND<500 Tnchlorofluoromethane ND<500 <br /> Dichlorodifluoromethane ND<500 1,2,3-Tnchloropropane ND<500 <br /> 1,1-Dichtoroethane ND<500 1,2,4-Tnmethylbenzen a 1600 <br /> t 1,2-Dichloroethane 1400 1,3,5-Tnmethylbenzene ND<500 <br /> 10-Dichloroethene ND<500 Vinyl Acetate " ND<500 <br /> cis-1,2-Dichloroethene ND<500 Vinyl Chloride(.) ND<500 <br /> trans-l,2-Dichloroethene ND<500 Xylenes,total 14,000 <br /> t 1,2-Dichloropropane ND<500 Comments <br /> 1,3-Dichloropropane ND<500 Surrogate Recoveries <br /> 2,2-Dichloropropane ND<500 DlbiomoflUOrOmethane 95 <br /> 10-Dichloropropene ND<500 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<500 4-Bromotluorobenzene 90 <br /> 'water and Napor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples i ug/L.,vapor samples 0 5 ug/L,solid and sludge samples 5 uglkg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (II 2-butanone, (g) 4-me1hyl-2- <br /> pentanone or isopropyl acetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />