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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> b9p//www mc�l cam E-mail main@mccampbcll corn <br /> Advanced GeoEnvironmental Client Project ID Larry's Auto Repair Date Sampled 11/22/99 <br /> 4005 North Wilson Way Date Received 11/23/99 <br /> IStockton, CA 95205 Client Contact Kevm McKibben Date Extracted 11/23-11/30/99 <br /> Client P O Date Analyzed 11/23-11/30/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 26118 <br />' Client ID VW-3111-22-99 <br /> Matrix . W <br /> Compound Concentration* Compound Concentration* <br /> Acetone roi ND<3600 trans-1,3-Dichloropropene ND<1000 <br /> Benzene 28,000 Ethylene dibromide NIK1000 <br /> Bromobenzene ND<1000 Ethylbenzene 3400 <br /> BTOmochlOTOmethane ND<1000 Hexachlorobutadiene ND<1000 <br />' Bromodichloromethane ND<1000 lodomethane ND<1000 <br /> Bromoform ND<1000 Isopropylbenzene ND<1000 <br /> Bromomethane ND<1000 p-Isopropyl toluene ND<1000 <br /> n-Butyl benzene ND<1000 Methyl butyl ketone ND<1000 <br />' sec-Butyl benzene ND<1000 Methylene Chlonde" ND<1000 <br /> tert-Butyl benzene ND<1000 Methyl ethyl ketone ND<1000 <br /> Carbon Disulfide ND<1000 Methyl isoburyl ketones ND<1000 <br /> Carbon Tetrachloride ND<1000 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<1000 Naphthalene ND<1000 <br /> Chloroethane ND<1000 n-Propyl benzene ND<1000 <br /> 2-Chlor00hyl Vinyl Ether` ND<1000 Styrene ND<1000 <br /> Chloroform ND<1000 1,1,1,2-Tetrachloroethane N D<1000 <br />' Chloromethane ND<1000 1,1,2,2-Tetrachloroethane ND<1000 <br /> 2-Chlorotoluene ND<1000 Tetrachioroethene ND<1000 <br /> 4-Chlorotoluene ND<1000 Toluene 17,000 <br /> Dibromochloromethane ND<1000 1,2,3-Tnchlorobenzene ND<1000 <br /> 1,2-Dibromo-3-chloropmpane ND<1000 12,4-Tnchlorobenzene ND<1000 <br /> Dibromomethane ND<1000 1,1,1-Trichloroethane ND<1000 <br /> 1,2-Dichlorobenzene ND<1000 1,1,2-Tnchloroethane ND<1000 <br /> 1,3-DlchloTobenzene ND<1000 Tnchloroethene ND<1000 <br />' 1,4-Dichlorobenzene ND<1000 Trichlorofluoromethane ND<1000 <br /> Dichlorodifluoromethane ND<1000 1,2,3-Tnchloropropane ND<l 000 <br /> 1,l-Dichloroethane ND<1000 1 2,4-Tnmethylbenzen a 1800 <br />' 1,2-1)ichlomethane ND<1000 1,3,5-Tnmethylbenzene ND<1000 <br /> 1,1-Dichloroethene ND<1000 Vinyl Acetate ND<1000 <br /> cis-1,2-Dichloroethene ND<1000 Vinyl Chloride ND<1000 <br /> trans-l,2-Dichloroethene ND<1000 Xylcncs,total 16,000 <br />' 1,2-Dichloropropane ND<1000 Comments <br /> 1,3-Dichloropropane ND<1000 Surrogate Reco%cries(%) <br /> 2,2-Dichloropropane ND<1000 Dibromofluoromethane 100 <br /> 1,1-Dichloropropene ND<1000 Toluene-d8 102 <br /> ns-1,3-Diehl oropropene ND<1000 4-Bromofluorobenzene 89 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and ail TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 us/!-,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,Hypes 0 2u&/wipe <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2 hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />