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2002 Soil Sampling <br /> In May 2002, LNC requested that I collect soil samples from the soil stockpile and determine if <br /> the soil could be removed to an offsite disposal site. I collected eight soil samples on May 13, <br /> 2002,at the locations depicted on Figure 2. The soil samples were submitted to Kiff Analytical <br /> LLC, (Kiff) of Davis, California for analysis. <br /> The soil samples were analyzed for TPH-mo and THP-d using USEPA Test Method 8015M and <br /> for Total Reportable Petroleum Hydrocarbons (TRPH)using USEPA Test Method 418.1. In <br /> addition,the samples were submitted through Kiff to Calscience Environmental Laboratories Inc. <br /> (CEL), Garden Grove, California, for analysis of CAM-17 metals. Copies of the analytical <br /> laboratory reports are presented in Appendix 1. <br /> Volatile organic compounds were not analyzed because as previous soil sample analytical <br /> laboratory results had not indicated their presence. <br /> Soil sample analytical reports indicated that the stockpile had petroleum hydrocarbon <br /> concentrations on May 13,2002 as follows: TPH-mo (850 to 2000 mg/kg); TRPH(290 to 790 <br /> mg/kg) (Table 1). No TPH-d was detected in the samples. A summary of the metals in the soil <br /> samples is presented in Table 2. CAM-17 metals were all reported to be below Total Threshold <br /> Limit Concentrations that would define hazardous waste (Table 3). <br /> 2006 Soil Sampling <br /> On January 9, 2006 and January 18, 2006 the soil stockpile was inspected and soil samples were <br /> collected. Pictures of the stockpile are shown in Appendix 2. Soil samples were collected as 4- <br /> point composite samples at three locations in the stockpile (Figure 2). The soil samples were <br /> analyzed for TPH-mo and TPH-d using USEPA Test Method 8015M. All of the soil samples <br /> were analyzed for VOCs using USEPA Test Method 8260B. <br /> Soil sample analytical results reported that the stockpile had petroleum hydrocarbon <br /> concentrations that ranged as follow: TPH-d(42 to 570 mg/kg); TPH-mo (140 to 1,300 mg/kg) <br /> (Table 1). These same soil samples were analyzed using USEPA Test Method 8260B for a full- <br /> scale of volatile organic compounds. No VOCs were detected above analytical method detection <br /> limits. <br /> A summary of the metals in the soil samples is presented in Table 2. CAM-17 metals were all <br /> reported to be below Total Threshold Limit Concentrations that would define hazardous wash <br /> (Table 3). <br /> Copies of the analytical laboratory reports are presented in Appendix 1. <br /> DAEnvironmentaI\LCN\LCN103.wpd 3 <br />