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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 1347 <br />12/22/2005 1414 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3384 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Analysis Batch: 720-3483 <br />d:\data\200512\122205\LCS <br />30.05 g <br />1 mL <br />d:\data\200512\122205\LCSD <br />30.04 g <br />1 mL <br />mg/Kg <br />12/21/2005 1435 <br />Analysis Batch: 720-3483 <br />Prep Batch: 720-3384 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3384/2-A <br />LCSD 720-3384/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />94101 10 - 130 7 35Dibenz(a,h)anthracene <br />Surrogate LCS % Rec LCSD % Rec Acceptance Limits <br />Nitrobenzene-d5 77 79 23 - 120 <br />2-Fluorobiphenyl 73 83 30 - 115 <br />Terphenyl-d14 83 98 18 - 137 <br />2-Fluorophenol 67 68 25 - 121 <br />Phenol-d5 74 74 24 - 113 <br />2,4,6-Tribromophenol 84 96 19 - 122 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 313 of 347