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Quality Control Results <br />Job Number: 720-1027-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/22/2005 2312 <br />12/22/2005 2341 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3384 <br />10 <br />10 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3483 <br />Analysis Batch: 720-3483 <br />12/21/2005 1435 <br />12/21/2005 1435 <br />Prep Batch: 720-3384 <br />Prep Batch: 720-3384 <br />d:\data\200512\122205\720-1 <br />30.10 g <br />5 mL <br />d:\data\200512\122205\720-10 <br />30.08 g <br />5 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1027-34 <br />720-1027-34 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />39 26 5 - 112 NC 35Phenol <br />48 44 12 - 158 NC 35Bis(2-chloroethyl)ether <br />46 40 23 - 134 14 352-Chlorophenol <br />45 37 9 - 172 NC 351,3-Dichlorobenzene <br />44 39 20 - 124 NC 351,4-Dichlorobenzene <br />11 0 10 - 130 NC 35 *Benzyl alcohol <br />43 42 32 - 129 2 351,2-Dichlorobenzene <br />49 51 10 - 130 4 352-Methylphenol <br />92 89 10 - 130 3 354-Methylphenol <br />48 47 9 - 230 NC 35N-Nitrosodi-n-propylamine <br />59 52 40 - 113 NC 35Hexachloroethane <br />60 53 35 - 180 14 35Nitrobenzene <br />67 65 21 - 196 3 35Isophorone <br />39 54 29 - 182 NC 352-Nitrophenol <br />67 57 32 - 119 NC 352,4-Dimethylphenol <br />59 54 33 - 184 9 35Bis(2-chloroethoxy)methane <br />62 53 10 - 130 NC 352,4-Dichlorophenol <br />70 66 44 - 142 6 351,2,4-Trichlorobenzene <br />67 62 21 - 133 NC 35Naphthalene <br />16 13 10 - 130 NC 354-Chloroaniline <br />76 64 24 - 116 17 35Hexachlorobutadiene <br />63 66 10 - 130 NC 354-Chloro-3-methylphenol <br />83 78 10 - 130 6 352-Methylnaphthalene <br />4 8 10 - 130 NC 35 **Hexachlorocyclopentadiene <br />60 68 37 - 144 12 352,4,6-Trichlorophenol <br />74 67 10 - 130 10 352,4,5-Trichlorophenol <br />73 81 10 - 130 11 352-Chloronaphthalene <br />72 62 10 - 130 14 352-Nitroaniline <br />78 82 9 - 112 5 35Dimethyl phthalate <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 314 of 347