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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11426-010-SA Date Extracted: 04-19-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-21-2018
<br />Client ID: SP2-10 Date Received: 04-05-2018 GC Column: DB5MS 2005 WHO TEQ: 1.08
<br />Matrix: Solid Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4479 % Solids: 92.69
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.170 - 0.0315
<br />1,2,3,7,8-PeCDD ND 0.244 -0.0468
<br />1,2,3,4,7,8-HxCDD ND 0.267 -0.0503
<br />1,2,3,6,7,8-HxCDD 0.772 - J 0.0772 0.0490 Total TCDD ND 0.170
<br />1,2,3,7,8,9-HxCDD 0.515 - J 0.0515 0.0488 Total PeCDD 0.350 -J
<br />1,2,3,4,6,7,8-HpCDD 15.3 -0.153 0.0541 Total HxCDD 5.24 -
<br />OCDD 132 -0.0396 0.0888 Total HpCDD 28.9 -
<br />2,3,7,8-TCDF 1.34 -0.134 0.0243
<br />1,2,3,7,8-PeCDF 0.313 - J 0.00939 0.0285
<br />2,3,4,7,8-PeCDF 0.758 - J 0.227 0.0298
<br />1,2,3,4,7,8-HxCDF 1.14 - J 0.114 0.0255
<br />1,2,3,6,7,8-HxCDF 0.933 - J 0.0933 0.0253
<br />2,3,4,6,7,8-HxCDF 0.617 - J 0.0617 0.0279
<br />1,2,3,7,8,9-HxCDF 0.453 - J 0.0453 0.0367 Total TCDF 7.51 -
<br />1,2,3,4,6,7,8-HpCDF 6.46 -0.0646 0.0321 Total PeCDF 5.33 -
<br />1,2,3,4,7,8,9-HpCDF 0.797 - J 0.00797 0.0396 Total HxCDF 7.31 -
<br />OCDF 8.97 - J 0.00269 0.0843 Total HpCDF 12.2 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 98.4 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 86.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 92.4 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 90.7 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 73.5 23.0 - 140
<br />13C-OCDD 60.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 101 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 82.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 82.7 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 94.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 96.8 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 95.2 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 95.3 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 80.1 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 89.7 26.0 - 138
<br />13C-OCDF 66.1 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 97.8 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/25/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/26/2018
<br />of 000020000014
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