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09 November 2021 <br />Project No. 21-6640 <br />Page 4 of 5 <br /> <br />3.1.2. Soil-Vapor Sampling & Analysis <br /> <br />At the proposed soil-vapor sampling locations, the borings will be advanced to 5 feet bsg <br />using hand tooling. Once the total depth is reached, semi-permanent soil-vapor sampling <br />wells will be installed within the boring. The temporary sampling points will consist of 7 <br />feet of ¼-inch Teflon tubing and a sampling tip (generally inert ceramic stone). Prior to <br />installing the tubing and sampling stone, #2/12 sand will be poured in the annuals of the <br />boring for the sample tip to rest on. The tubing and sampling tip will then be lowered to a <br />depth of five feet bsg and one foot of #2/12 sand will be poured around the tip to create <br />a filter pack. Above the sand, one foot of dry granular bentonite will be placed to a depth <br />of 4 feet bsg. Thereafter, hydrated bentonite will be placed from 3 feet bsg to near surface <br />grade to seal each location and prevent ambient air intrusion during sampling. <br /> <br />A soil-vapor sample will be collected after allowing a minimum of two hours equalization <br />time following installation of the soil-vapor wells. Prior to soil-vapor sample collection, <br />three calculated volumes of air will be purged utilizing a 6-liter purge canister or pump, <br />calibrated to 200 milliliters per minute (ml/min). One-liter Summa® sampling canisters will <br />be used to collect soil-vapor samples for VOC/TO-15 analysis. <br /> <br />The sampling inlet manifold consists of a vapor-tight valve; a particulate filter; a flow <br />restrictor calibrated to 200 milliliters per minute (ml/min). The manifold assembly will be <br />attached to the ¼-inch Teflon® tubing from the soil-vapor well. <br /> <br />The canister’s initial vacuum will be measured and recorded between -26 and -30 inches <br />of mercury (in hg). Shut-in tests will be performed on each assembly by attaching and <br />securing the sample and purge canisters to the manifold and opening the valves on the <br />purge canister and the manifold. The shut-in test is performed for approximately 10 <br />minutes on each assembly. <br /> <br />The soil-vapor point will be isolated from ambient air by enclosing the borehole, tubing <br />and manifold/canister assembly in a 100-liter shroud. Helium will be emitted into the <br />shroud surrounding the well borehole, tubing and manifold/canister assembly and acts as <br />a tracer gas to evaluate if leaks in the sampling apparatus have allowed infiltration of <br />ambient air. <br /> <br />Upon achieving a successful leak test, the purge canister valve will be opened for a period <br />to allow the three calculated volumes of air to be purged. The purge vacuum gauge will <br />be monitored to ensure a proper decrease of vacuum purged. <br /> <br />Upon achieving the targeted purge volume, the sample canister valve opened. The initial <br />pressure and time are recorded. Upon reaching at least -5 in Hg or less, the sample <br />canister valve will be closed, and final pressure and time recorded. The sampling port on <br />the sampling canister will be capped with a brass end-cap. <br />